Isolation of amygdalin epimer at high diastereomeric purity and its structural characterization by spectroscopic and Q-TOF LC-MS methods

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dc.contributor.authorSabir, Pshtiwan Raheem
dc.contributor.authorCapan, Irfan
dc.contributor.authorAysal, Ayhan Ibrahim
dc.contributor.authorServi, Suleyman
dc.date.accessioned2026-08-12T17:06:47Z
dc.date.issued2021
dc.departmentFırat Üniversitesi
dc.description.abstractAmygdalin, a cyanogenic glycoside mostly found in the bitter almond kernel, plays an important role in conventional and modern medicine applications. The high diastereomeric purity amygdalin was isolated with chromatographic purification methods and recrystallization. Amygdalin and neoamygdalin were separated chromatographically using the porous graphitic carbon column. Identification and confirmation of each molecule was performed with the ESI Quadrupole Time of Flight system coupled with a reversed phase LC.
dc.description.sponsorshipFrat University Research Project Coordination Unit [FF.19.03]
dc.description.sponsorshipWe would like to thank Frat University Research Project Coordination Unit (Project Number FF.19.03) for the financial support of this study.
dc.identifier.doi10.25135/jcm.60.2105.2076
dc.identifier.endpage185
dc.identifier.issn1307-6183
dc.identifier.issue2
dc.identifier.orcid0000-0002-9555-1555
dc.identifier.scopus2-s2.0-85124762382
dc.identifier.scopusqualityQ3
dc.identifier.startpage172
dc.identifier.trdizinid509814
dc.identifier.urihttps://doi.org/10.25135/jcm.60.2105.2076
dc.identifier.urihttps://search.trdizin.gov.tr/tr/yayin/detay/509814
dc.identifier.urihttps://hdl.handle.net/11508/49400
dc.identifier.volume15
dc.identifier.wosWOS:000730436500001
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.indekslendigikaynakTR-Dizin
dc.language.isoen
dc.publisherAcg Publications
dc.relation.ispartofJournal of Chemical Metrology
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/openAccess
dc.snmzKA_WoS_20260511
dc.subjectAmygdalin
dc.subjectneoamygdalin
dc.subjectcyanogenic glycoside
dc.subjectLC-MS Q-TOF
dc.subjectchromatography
dc.titleIsolation of amygdalin epimer at high diastereomeric purity and its structural characterization by spectroscopic and Q-TOF LC-MS methods
dc.typeArticle

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